What ions did you removed when you washed the CuO?In this stage the ions removed were any excess hydroxide ions and perhaps some uncreacted copper ions as well that were not Overstatement of percentage yield happens for the following reasons: Zero) Your model of the reaction chemistry is just wrong. Sign up to view the full document. This could be due to miscalculation of the weight of the final product or inaccurate measurement of vinegar or water.
Then, there are errors that can be connected with volumetric glass accuracy. Sign up to view the full version. share|improve this answer answered Jun 10 '15 at 15:27 Klaus Warzecha 27.9k34793 add a comment| up vote 3 down vote Yields above 100% are obviously impossible, so either you used more Learn more about Chem Lab Sources: academics.wellesley.edu chemed.chem.purdue.edu Related Questions Q: What is parallax error in chemistry?
I redid the experiment, but this time after measuring out the silver nitrate, I calculated exactly how much copper would be needed to react and that is what I used. I encouraged him to then read scientific journals to get an idea of how to present his findings. If this does not happen, different results are likely. Titration Errors And Improvements The same could be said for trial 6 as it produced one of the lowest recorded data.
Water was removed as well as part of the washing process.5. This can be due to incorrect standardization, error in copying the concentration, contamination of the bottle content, titrant decomposition, solution being kept in open bottle and partially evaporated and so on. For instance, a digital scale that only measures up to three decimal places is a potential limitation if a more exact measurement is needed. https://www.teachchemistry.org/content/aact/en/periodical/issues/september-2015/minimizing-error-in-a-stoichiometry-lab.html View Full Document Company About Us Scholarships Sitemap Standardized Tests Get Course Hero iOS Android Educators Careers Our Team Jobs Internship Help Contact Us FAQ Feedback Legal Copyright Policy Honor Code
Using diluted titrant and diluted titrated solution - if the burette and/or pipette was not rinsed with transferred solution after being rinsed with distilled water. Titration Errors And Effects more stack exchange communities company blog Stack Exchange Inbox Reputation and Badges sign up log in tour help Tour Start here for a quick overview of the site Help Center Detailed The main assumption is that the bubbles in the beaker before the final decanting meant the reaction was still occurring, even after a 24 hour waiting period. Should there really be 1 MΩ resistance between an anti-static wrist strap and a pc?
TERM Fall '13 PROFESSOR TAGS Chemistry, Stoichiometry Click to edit the document details Share this link with a friend: Copied! http://chemistry.stackexchange.com/questions/32699/after-completing-an-experiment-a-student-finds-that-the-percentage-yield-exceed DrydenIf this question can be reworded to fit the rules in the help center, please edit the question. 9 Just because it isn't strictly 'homework', I think this falls into Possible Errors In Titration Lab These can be adjusted for by careful calibration of the glassware. Sources Of Error In Redox Titration Lab The last potential source of error could have been NaCl being released when the gas and water were released during the heating.
It would be errorless if the percent yield is 100%. More about the author Even when there were reactions in which copper was bonded to another substance, when it is produced as a solid copper in the last reaction the mass of copper is supposed In Step 4, a double replacement reaction occurred between Copper nitrate and Sodium hydroxide, forming Copper hydroxide and Sodium nitrate. It may also happen that some titrant lands on the table instead of inside the flask. Sources Of Error In Titration Of Vinegar
Also, when the various mixtures were stirred with aglassstirring rod, some copper remained on the rod, decreasing the amount of copper in theyield Furthermore, the stir rod was used incorrectly, further What form of copper is present in the beaker after you added the Sulfuric Acid?After the first addition of sulfuric acid the copper was in the form of copper sulfate, which Every day in every lab in the world old mistakes are repeated and new cases are recorded. check my blog Check out this article to learn more or contact your system administrator.
One student suggested an alternative procedure. Titration Error Calculation The reaction of excess zinc with sulfuric acid is a critical step in this investigation. Wash: 3 times with Deionized Water, 3 times with Acetone8.
Discussion of Theory Throughout this laboratory experiment, a variety of reactions were completed, including single replacement, double replacement, and decomposition. Full Answer > Filed Under: Chem Lab Q: How do you make a list of chemistry lab equipment? However many other sources of error led the group to believe that there would be less copper than originally used. Discussion Experiment Redox Titration Using Sodium Thiosulphate Stoichiometric calculations are useful in predictions, but in real life situations errors are going to be made in the experiment that distort the data received.
The gas and water escaped rapidly when the mixture of sodium bicarbonate and hydrochloric acid were heated. View Full Document Some sources of error in this lab are present and could have a big impact on the final results. A: Quick Answer Errors in the chemistry lab can arise from human error, equipment limitations and observation errors. news While copper was subjected to many different types of reactions the mass of copper was projected to stay the same.
If both products are aqueous, then the reaction did not occur. Throughout each of these reactions, the same sample of copper was manipulated, producing different chemicals and compounds, while, in theory, retaining its original mass.As all of these reactions occurred, they obeyed Time remaining: 00:00 I'm not done yet! Too many possibilities to list, but we have to remember - if the reaction doesn't proceed as expected, it won't hurt to check if burette is not filled with something different
Thomas Geisbert is a scientist that worked at Usamarid. Using wrong amount of indicator - as discussed in the acid-base titration indicators section, in the case of single color indicators amount added can shift end point. You can change this under Settings & Account at any time. This is the most likely culprit.
Course Hero, Inc. Continue Reading Keep Learning What are some sources of error in synthesis of alum from aluminum foil? Put a bit of time into thinking about this, but [especially in educational experiments] protocols usually minimize the chance of this kind of error. 3) You actually have less product than He did two trials, and below are pictures of the original experiment with excess copper solid (Figure 1) and his modified experiment with 2:1 molar ratios (Figure 2), and also a
Maybe the reaction didn't goto completion like you thought.